以杨木为研究对象,采用单一因素法研究了杨木初含水率,微波辐射时间及微波辐射功率对杨木活性染料染色效果的影响规律,获得较优的杨木微波预处理工艺。结果表明:(1)微波预处理可以破坏木材内部微观结构,改善木材渗透性;(2)随着杨木初含水率的升高,上染率逐渐下降。当初含水率为25%时,其上染率和固色率分别为39.44%和38.31%;(3)随着微波辐射时间的延长,上染率和固色率均呈上升趋势,当辐射时间为90 s时,与未处理木材相比上染率可提高21.15%,固色率可提高21.44%;(4)随着微波辐射功率的增大,染色效果也更佳;当辐射功率为18 k W时,与未处理木材相比上染率可提高21.38%,固色率可提高21.59%。
Anodic electrodes with the mixture of hydrogen storage alloys and different contents of Co3O4（2%,4%,6% and 8%,mass fraction） powders were made.The effects of Co3O4 on the electrochemical performance of the alloy electrodes were studied.The constant charge-discharge tests show that the discharge capacity of alloy electrodes with Co3O4 significantly increases,and the maximum discharge capacities of electrodes with 2%,4%,6% and 8% Co3O4 are higher than the electrode with no Co3O4 by 0.83%,4.86%,7.18% and 9.21%,accordingly.Linear polarization（LP） and electrochemical impedance spectroscopy（EIS） tests suggest that charge-transfer resistance decreases by the addition of Co3O4.Cyclic voltammogram（CV）,scanning electron microscopy（SEM） and energy dispersive spectrum（EDS） tests indicate that Co3O4 can partly dissolve and experience a reversible oxidation-reduction process of Co to Co（OH）2,leading to the improvement in the electrochemical performance of hydrogen storage alloy.
