High entropy alloy has attracted increasing attentions.However,to enhance the alloy strength often leads to impairment of the ductility,or vice versa.Here we reported a heat treatment approach on AlCrFeNi2Ti0.5 high entropy alloy,which can elevate the strength and ductility simultaneously.An ingot of AlCrFeNi2Ti0.5 weighing 2.5 kg was firstly fabricated by medium frequency induction melting.Then samples from the same height of the bulk ingot were annealed for 6 h at 600,700,800 and 1000 ℃,respectively.After 1000 ℃ annealing,an optimal microstructure was obtained by using our approach which can make some precipitation particles distribute homogeneously in the dendrite interior while keep the interdendrite structure as a single solid solution phase.The mechanical test on this AlCrFeNi2Ti0.5 alloy sample showed that,the compressive fracture strength σbc was increased by about600 MPa and the plastic strain ep was doubled,compared with those of the as-cast sample.Our approach can be readily adapted to large-scale industrial production of high entropy alloys with high strength and ductility by proper annealing treatment.
Li JiangHui JiangYiping LuTongmin WangZhiqiang CaoTingju Li
Zn-Al-Cu-TiB2(ZA27-TiB2) in situ composites were fabricated via reactions between molten aluminum and mixed halide salts(K2TiF6 and KBF4) at temperature of 875 °C. The microstructure, mechanical properties and wear behavior of the composites were investigated. Microstructure analysis shows that fine and clean TiB2 particles distribute uniformly through the matrix. The mechanical properties of the composites increase with the increase in TiB2 content. As TiB2 content increases to 5%(mass fraction), an improvement of HB 18 in hardness and 49 MPa in ultimate tensile strength(UTS) is achieved. The overall results reveal that the composites possess low friction coefficients and the wear rate is reduced from 5.9×10-3 to 1.3×10-3 mm3/m after incorporating 5% TiB2. Friction coefficient and worn surface analysis indicate that there is a change in the wear mechanism in the initial stage of wear test after introducing in situ TiB2 particles into the matrix.